Fourth DONES Users Workshop
Main Auditorium
CIEMAT

We kindly invite all interested members of the scientific and engineering community to participate in the Fourth IFMIF-DONES Users Workshop.
The workshop will be held as an in-person event in Madrid, Spain on October 13-15, 2026 at the CIEMAT research center, organized jointly by esDONES and CIEMAT.
As the construction of the DONES facility progresses, the objective of this DONES User´s Workshop is to review the research areas of DONES, discuss and further detail the experimental programme and consolidate the users community. In particular, the leading motive of the Fourth Workshop will be to propose key-experiments that could profit from the already proposed extensions of DONES baseline associated with its experimental capabilities, in particular, the addition of the second accelerator, post irradiation examination facilities, TOF-DONES facility, collimated neutron beam facility.
One of the main roles for the DONES Users Community is to establish a stable link of communication between the DONES engineering activities and the future users. This is to ensure that requirements coming from the proposed experiments are properly evaluated in terms of technical feasibility, ease of implementation and available budget and factored in during the construction phase of the facility.
Areas of scientific interest / sessions of the workshop:
- Qualification of materials for the fusion programme, DEMO and fusion power plant
- Tritium breeding technologies: validation at DONES
- Studies of functional materials and other fusion technologies
- Experiments for benchmarking of computational materials science
- Nuclear physics: TOF-DONES facility and other experiment
- Industrial neutron irradiations and societal applications
- Life sciences and medical applications
- Experiments during the commissioning phase of DONES
- Discussion of the DONES experimental programme proposal
- DONES users community: presentation of the Users Committee members and future activities
The program of the sessions will be composed of a small number of introductory key-note talks and several presentations selected based on submitted abstracts. We kindly invite you to send abstracts and contribute to the workshop. Participation of young researchers is encouraged.
Deadline for submission of abstracts is 22 June 2026.
The authors of talks selected for presentation will be notified by 7 July 2026.
The participants will be asked for a 170 Euro registration fee to cover the cost of lunches at CIEMAT, a workshop dinner and coffee breaks.
Early registration and payment deadline is 30 September 2026.
Please register as a member of the DONES users community if you wish to receive updates on the DONES Users workshop.
We are looking forward to your contributions and participation.
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Registration Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid -
Opening and introductory session Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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Welcome from CIEMAT management
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Workshop practical information
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Overview of the DONES Programme
IFMIF-DONES (International Fusion Materials Irradiation Facility, DEMO-Oriented Neutron Early Source) is a cutting-edge neutron irradiation facility designed for the study and qualification of materials intended for use in fusion reactors. It also contributes to the development of tritium and breeding blanket technologies. As part of the European roadmap to fusion electricity, its primary objective is to create a comprehensive database of material properties under intense neutron irradiation conditions, similar to those encountered in a fusion reactor. The neutron source is generated by an accelerated deuteron beam striking a liquid lithium curtain, producing neutrons with an energy spectrum and flux comparable to those experienced by the first wall of a fusion reactor.
The IFMIF-DONES facility has moved from the preliminary design to the detailed design phase, with some components already in production. The construction phase officially began with the first DONES Steering Committee on 16 March 2023, ensuring a smooth transition of design activities handover to the DONES Programme Team. This paper summarizes the current status of the DONES Programme and the IFMIF-DONES design.
The focus will be on the design status of the DONES Facility and its Accelerator Systems, which are designed for delivering the 5 MW D+ beam at 40 MeV with high availability. Additionally, it will provide an update on the status of hardware procurement through the In-Kind Contribution of the engaged parties and include an overview of the facility's experimental capabilities.
Ponente: Philippe Cara (F4E) -
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IFMIF-DONES design and construction statusPonente: Moises Weber (IFMIF-DONES España)
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Assessment of the IFMIF-DONES irradiation capabilities
International Fusion Materials Irradiation Facility—DEMO Oriented Neutron Source (IFMIF-DONES) is a research facility primarily designed for the investigation and qualification of materials for future fusion reactors. To this end, IFMIF-DONES has been designed to achieve material damage levels equivalent to those expected in the walls of future fusion reactors. Beyond its primary mission, the intense neutron fields generated by the accelerator also offer significant opportunities for a wide range of complementary scientific and technological applications, whether related to fusion environments or to other research fields. This work presents an analysis of the neutron fluence rate obtained in the Test Cell area and in other complimentary experimental rooms. The sensitivity study was carried out by varying the number of modules installed in the Test Cell area and considering operating scenarios with one or two accelerators. So far, the modules considered in the Test Cell area are the High Flux Test Module (HFTM) and the Tritium Breeder Unit (TBU). The results provide valuable insights into the optimization of IFMIF-DONES operation and its capability to support a wide range of scientific and technological activities.
Ponente: Irene Álvarez Castro (Consorcio IFMIF-DONES España)
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Coffee break
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Nuclear physics: TOF-DONES facility and other experiments Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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Presentation of TOF-DONES
TOF-DONES is a high intensity neutron time-of-flight facility designed for IFMIF-DONES. The idea is to extract, in a pulsed way, 0.1% of the deuteron beam and send it to room R026. There, the deuteron pulses will impact a target, possibly made of graphite or berillium, generating neutrons. These neutrons will then travel along different time-of-flight beam lines in vacuum to the experimental areas. The objective of the installation is to perform neutron measurements of interest to fission and fusion technologies, astrophysics, medical physics, nuclear structure, dosimetry, and other fields.
In this workshop we will present the preliminary design of TOF-DONES, completed in the context of the DONES Consolidation Phase 1 project (2023-2025), including the description of the neutron converter, the different beam lines, shieldings, collimators... and the characteristics of the neutron beam in the different experimental areas.
Ponente: Emilio Mendoza Cembranos (CIEMAT) -
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The n_TOF Facility at CERN: A Quarter Century of Unique Contributions to Neutron Physics
In this contribution, the n_TOF facility at CERN will be presented, with emphasis on the unique characteristics that make it a leading neutron time-of-flight facility worldwide.
The integration of n_TOF within the CERN ecosystem and the strategic advantages this positioning offers will be discussed, including access to world-class infrastructure, expertise, and collaborative networks. During the quarter century of operation, highly specialized and well-tailored experimental setups have been developed, optimized for precision measurements across a broad-energy range. More recently, advances in detector R&D and newly established experimental techniques have further enhanced the measurement capabilities of the Collaboration, opening exciting new physics avenues. In this talk, the most important setups and techniques developed at n_TOF will be highlighted.
The n_TOF Collaboration is, since the beginning, the largest neutron physics collaboration globally, continuously attracting new participants over the years, reflecting the facility's central role in the field. Selected achievements demonstrating the facility's impact on nuclear data for applications ranging from nuclear energy to astrophysics will be presented.
Finally, the general principle that critical measurements for emerging nuclear technologies and other applications benefit from independent verification at multiple facilities will be addressed. In this context, potential areas where complementary measurements between established facilities like n_TOF and future facilities could serve the broader nuclear physics community will be briefly discussed.
Ponente: Prof. Nikolaos Patronis (CERN & University of Ioannina - Greece) -
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Key Nuclear Data Needs for Fusion Applications: A Selective Review
Nuclear data underpin the design and analysis of fusion systems. Nuclear analyses provide key performance metrics — tritium production, heat deposition, material irradiation, and radiation distributions — through simulations based on fusion-relevant nuclear data, including neutron transport, activation, and displacement cross sections, and gas production data. This talk offers a review of existing nuclear and experimental data for fusion applications, focusing on the critical cross sections governing tritium production, neutron multiplication, material damage, and gas production, as well as dosimetry data for detectors of key elements and materials. Drawing on current fusion-specific libraries (e.g., FENDL-3.2, JEFF-4, TENDL-2025) and additional recommended nuclear data, we identify remaining nuclear data development needs and experimental needs and discuss the potential of time-of-flight (TOF) facilities to deliver the high-quality data, which is required to support the coming decade of fusion development.
Ponente: Dr. Yuefeng Qiu (Karlsruhe Institute of Technology) -
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Scintillator-based fast neutron diagnostics systems and neutron/gamma discrimination studies at the ToF-DONES
The Radiation Detectors and Plasma Diagnostics Division at the National Centre for Nuclear Research has been conducting research on scintillation detectors for neutron–gamma discrimination for over two decades. The team’s recent work included characterization of the Organic Glass Scintillator (OGS) and evaluation of its neutron–gamma discrimination performance compared to organic scintillators EJ-276, EJ-309, M600, and stilbene [1]. While single-crystal stilbene still provides the best overall discrimination, OGS is a strong competitor. Parallel studies examined the effect of light self‑absorption on pulse-shape discrimination in OGS samples of different sizes [2], and these effects are taken into account when scaling detector dimensions. In 2023, extensive studies were conducted on a novel polyurethane-based plastic scintillator, M600, and compared with the classic EJ-200 [3]. M600 proved to be a durable and cost-effective material for radiation detection in harsh environments, offering reliable neutron–gamma separation and increased resistance to ageing and humidity. Thanks to the group’s long-standing expertise, the NCBJ team is actively participating in the construction of the Vertical Neutron Camera (VNC) for the JT-60SA tokamak in Japan. At the workshop, a short presentation will be given on building neutron diagnostics for ToF-DONES and on performance tests of new scintillator compositions to be conducted using neutron beams at ToF-DONES.
[1] M. Grodzicka-Kobylka et al. Nucl. Instr. Meth. A Vol. 1077 (2025) 170559, DOI: 10.1016/j.nima.2025.170559
[2] L. Adamowski et al. ArXiv Vol. 2504.11963 (2025) 1-21, DOI: 10.48550/arXiv.2504.11963
[3] A. Syntfeld-Każuch et al. Nucl. Instr. Meth. Phys. Res. A Vol. 1068 (2024) 169764, DOI: 10.1016/j.nima.2024.169764Ponente: Dr. Agnieszka Syntfeld-Kazuch (National Centre for Nuclear Research (NCBJ))
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Visit to the TJ-II stellerator (t.b.c.) Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid
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Experiments for benchmarking of computational materials science Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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Multiscale models for materials and DONES: microstructural observables, environmental conditions, and interpretation of observations
Sergei L. Dudarev
UK Atomic Energy Authority, Culham Campus, Abingdon, Oxfordshire OX14 3DB, United Kingdom
Department of Materials, University of Oxford, Parks Road, Oxford OX1 3PH, UK
Multiscale models for nuclear materials have now become sufficiently advanced to enable simulations of microstructures of irradiated materials at the level of fidelity, where predictions, derived from models involving no adjustable parameters, can be quantitatively compared with experimental observations. Defect and dislocation microstructures predicted by simulations, have recently been compared with transmission electron microscopy images, X-ray diffraction, Rutherford backscattering spectroscopy and hydrogen desorption spectroscopy measurements, producing surprisingly favourable outcomes. The results extended beyond the interpretation of observations, leading to fundamentally new insights into microstructural processes driven by impacts of energetic particles. Models for radiation effects have also been extended to reactor component scale, providing a foundation for the holistic assessment of materials performance in an operating fusion power plant.
The availability of an intense source of neutrons, with the spectrum matching that of the D-T fusion plasma, provides new opportunities for testing and developing materials, extending the capabilities provided by ion and fission irradiation experiments and broadening the range of testing conditions, to match the fusion power plant conditions. Full tokamak simulations are already able to define the spectrum of mechanical stress and irradiation doses expected at various spatial locations in an operating fusion tokamak, with further effort aiming at providing a quantitative definition of dynamically evolving space of operating conditions for materials in a fusion device. Presently available literature data provide only highly approximate estimates, whereas engineering design studies require a database detailing the evolution of materials in a multi-dimensional space of environmental variables including the neutron irradiation dose rate, time, temperature, tensorial stress, hydrogen isotope atmosphere, generation of transmutation elements, interaction with coolants, corrosion, occurrence of transients etc.
The presentation outlines the areas, where combining DONES capabilities with predictive materials simulations might prove most impactful, offering a comprehensive view of materials testing and validation, linked to reactor design studies and involving the assessment of data derived from complementary ion irradiation and fission reactor irradiation experiments.
Ponente: Sergei Dudarev (UKAEA and University of Oxford)
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Qualification of materials for the fusion programme, DEMO and fusion power plant Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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EUROfusion material development and qualification roadmap for baseline and advanced materials for fusion in-vessel components
The first objective of the EUROfusion Work Package Materials is the characterization and qualification of the three baseline materials, i.e. EUROFER97 steel for blankets and divertor cassette structure, tungsten as plasma facing armor material, and copper-chromium-zirconium (CuCrZr) for divertor heat-sinks. Qualification of the industrially available baseline materials, up to a level sufficient for nuclear licensing, is pursued by means of experimental testing and characterization activities before and after exposure to fusion reactor relevant neutron irradiation conditions with strong emphasis on traceability and quality assurance. This also comprises the preparation for neutron irradiation campaigns to be performed in IFMIF-DONES, by the qualification of testing methods and definition of testing standards.
The second objective is the development, characterization and industrialization of few risk-mitigation alternative structural, heat-sink and plasma-facing materials with improved operational performance - i.e. radiation resistance, increased design window and/or other risk minimizing features. This is an essential part of the risk-mitigation strategy towards a Fusion Power Plant, in case baseline materials would not meet future operational requirements. This requires substantial involvement from industry partners and the qualification of the materials under neutron irradiation in parallel to the activities performed for the baseline materials.
The third pillar concerns the selection, characterization and qualification under operation relevant neutron loading conditions of functional materials, i.e. optical and dielectric materials for diagnostics and H&CD as well as insulator materials for breeding blanket and divertor applications.
Tracking of the advancement of material maturity is done by the assessment of the Materials Technology Readiness Level (MTRL) with the aim to advance material maturity to level 7 (System prototype demonstration in an operational environment). Thereby, baseline materials currently exhibit maturity levels between 4-5 where system integration issues become increasingly important. Therefore, maturation of materials to level 7 cannot only be done by tests using basic material specimens but also is dependent on the maturation of the system for which it will be used. The actual roadmap towards MTRL 7 will be sketched and existing obstacles and time-constraints outlined.Ponente: Gerald Pintsuk (FZJ) -
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Small Specimen Test Technique to investigate neutron irradiation effects: development performed within EUROfusion project in 2021-2025
D. Terentyev1,2, E. Gaganidze3, Mario Walter3, M. Carrington4, K. Amjad4, D. Cinger5, A. Zinovev1, D. Bermudez1,6, M. Serrano7, R. Hernandez7, R. Molak8, G. Pintsuk9, G. Aiello10
- Belgian Nuclear Research Centre, SCK CEN, Mol, 2400, Belgium
- Ghent University, Department of Materials, Textiles and Chemical Engineering, Ghent, Belgium
- Karlsruhe Institute of Technology (KIT), Institute for Applied Materials, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen, Germany
- United Kingdom Atomic Energy Authority, Culham Centre for Fusion Energy, Culham Science Centre, Abingdon, Oxon OX14 3DB, UK
5 HUN-REN CER, KFKI Campus, 1121, Budapest, Konkoly-Thege Miklós út 29-33, Hungary
6 Institute of Mechanics, Materials and Civil Engineering, UCLouvain, 1348 Louvain-la-Neuve, Belgium - CIEMAT. Avd. Complutense 40, 28040 Madrid, Spain
- Warsaw University of Technology, Faculty of Materials Science and Engineering, Wołoska 141,
02-507 Warsaw, Poland - Forschungszentrum Jülich GmbH, Institute of Fusion Energy and Nuclear Waste Management – Plasma Physics, 52425 Jülich, Germany
- EUROfusion PMU, Boltzmannstraße 2, 85749, Garching, Germany
Within the EUROfusion programme, the Work Package “Materials”, among various objectives, pursues the development of validation of so-called “Small Specimen Test Techniques” (SSTT) to enable cost-efficient use of irradiation facilities. The main issue to be resolved is to elaborate a prudent approach for the inclusion of the sub-sized geometries of specimens, which are currently out validity range or not specified in the existing test standards. Six labs are contributing to this subject, focussing the efforts on:
(i) review on the currently available SSTT methods and samples geometries used in previous programmes;
(ii) identify and propose small size geometries for tensile, fatigue, creep and fracture tests;
(iii) execute experimental programs to validate (minimum) allowable size and transferability of the properties extracted using SSTT;
(iv) prepare the guidelines (and recommendations) to establish the basis for a standard of “fusion specific SSTT”;
(v) execute Pilot Run and Interlaboratory study on down-selected test configurations.This contribution presents an overview of the current status, example of achieved tasks and near-term action plan.
Ponente: Dmitry Terentyev -
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Pre-Qualification of Small-Scale Tensile Testing Methodologies for EUROFER97 and CuCrZr Towards Future IFMIF-DONES Irradiation Campaigns
The qualification of structural and functional materials for fusion reactors requires extensive mechanical testing under neutron irradiation. However, the limited irradiation volume available in current facilities and in future neutron sources such as IFMIF-DONES makes the use of conventional tensile specimens impractical. Small Specimen Test Technology (SSTT) has therefore emerged as a key approach for maximizing the amount of mechanical information obtained from irradiated material volumes. Nevertheless, the reduced dimensions of these specimens raise questions regarding transferability and the equivalence of the measured properties with respect to standard-sized specimens.
Within the framework of a EUROfusion Engineering Grant, an ongoing interlaboratory programme is being conducted to validate miniature tensile testing methodologies for two fusion-relevant materials: EUROFER97 and CuCrZr. The study includes several SSTT geometries, namely the European EUFLAT, the Japanese SSJ3, and the SCK-CEN cylindrical tensile specimen geometry, tested at different laboratories and temperatures. Particular attention is devoted to the development of robust testing procedures, specimen metrology, machine compliance correction and data processing methodologies, together with the assessment of the influence of microstructure, grain size, specimen dimensions and surface roughness on the reproducibility and transferability of key tensile properties such as yield strength, ultimate tensile strength and elongation.
The ultimate objective of this work is to contribute to the qualification of SSTT methodologies that can be reliably applied to future irradiated materials campaigns. The results obtained will support the future exploitation of IFMIF-DONES by providing validated mechanical testing procedures capable of extracting meaningful tensile properties from the limited material volumes available after irradiation. In this sense, the work represents a necessary step towards the generation of qualification data for fusion structural and high-heat-flux materials under representative irradiation conditions.Ponente: Francisco Canillas (CIEMAT - National Fusion Laboratory)
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Coffee break
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Qualification of materials for the fusion programme, DEMO and fusion power plant Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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Fracture Data Acquisition Approach for Reliability Assessment of RAFM Steel in Fusion DEMO Reactors
The qualification assessment of low-activation ferritic-martensitic steel (RAFM), a key structural material for fusion DEMO reactors, is a critical challenge for the realization of such reactors. The IFMIF-DONES program identifies the acquisition of neutron irradiation data as a key strategy to support this qualification assessment. The design of future in-vessel components will be verified according to structural design codes that have not yet been fully established. In particular, non-inspectable regions are expected to be evaluated through probabilistic fracture analysis based on hypothetical defects. Therefore, the application of probabilistic risk assessment (PRA) incorporating the statistical distribution of fracture characteristics is essential. This approach requires reliable fracture toughness and strength data that capture material variability under relevant conditions. In this study, we present a framework for acquiring such fracture mechanics data using small-scale specimen technology, which is particularly advantageous
Ponente: Dr. Takashi Nozawa (National Institutes for Quantum Science and Technology) -
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Bridging the Gap: Fusion-Fission Synergies to Accelerate Material Qualification for DEMO and Fusion Power Plants
Future fusion power systems will expose materials to some of the harshest operating conditions ever considered in nuclear engineering, combining intense neutron irradiation, helium production, thermal cycling, high temperatures, and chemically aggressive environments. While fusion introduces unique challenges, many of the underlying degradation mechanisms and qualification needs are closely connected to those already faced in advanced fission systems. This creates a strong opportunity for deeper collaboration between fusion and fission materials communities. This contribution discusses how shared approaches to materials qualification can help accelerate the deployment of both future fusion reactors and advanced nuclear systems. In particular, it highlights recent efforts within European collaborative initiatives such as CONNECT-NM to develop integrated methodologies for the qualification of materials under extreme environments. Key topics include the development of structured experimental test-beds, accelerated screening and qualification routes, and multi-scale experimental platforms capable of reproducing complex irradiation and thermo-mechanical conditions. The role of major irradiation infrastructures, especially IFMIF-DONES, is discussed in the context of bridging the gap between laboratory materials development and reactor-relevant qualification. The contribution also explores emerging approaches for materials health monitoring based on advanced non-destructive examination and testing techniques, combined with physics-based modelling, data-driven methods, and AI-assisted analysis. These digital approaches, together with interoperable “smart” databases for nuclear materials, can support more predictive and adaptive qualification strategies for both fusion and fission applications. Overall, the presentation aims to highlight how fusion–fission synergies can significantly shorten qualification timelines, improve confidence in materials performance, and strengthen the scientific foundations needed for the next generation of nuclear energy systems.
Ponente: Prof. Marta Serrano Garcia (CIEMAT) -
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Materials selection for the DONES High Flux Test Module
The DONES High Flux Test Module shall serve to irradiate material samples up to 50 dpa in a temperature range of 250 - 550 °C in a 14 MeV type neutron spectrum. Inevitably, the same and even slightly higher structural damage will be effected in the HFTM's structural and functional components. The HFTM design responds to this challenge by separation of functions and avoiding the most critical combination of loads (i.e., adjusting temperature and stresses in a beneficial way) where possible. Still, the pressure bearing container of the HFTM is challenged by swelling and loss of ductility, the capsules at low temperatures could face embrittlement, and the ceramic insulators of the electrical heaters and sensors are affected by Radiation Induced Conductivity and Radiation Induced Electrical Degradation. The contribution discusses quality and magnitude of the effects, measures to mitigate detrimental effects in the design of the HFTM, and steps towards an optimized materials selection.
Ponente: Frederik Arbeiter (KIT) -
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Development Challenges for Tungsten-Based Materials and Joints Under Fusion-Relevant Neutron Loading in Plasma-Facing Components
A key challenge in the development of magnetic confinement fusion power plants is the reliable exhaust of heat and particles. Divertor plasma-facing components (PFCs) must therefore withstand extreme thermal and particle loads, including neutron irradiation, which progressively degrades critical material properties. Current divertor PFC concepts typically rely on a monolithic tungsten (W) armor joined to a copper (Cu) alloy heat sink. This architecture combines the plasma compatibility of tungsten with the high thermal conductivity of a copper-based heat-sink structure. Ensuring the thermomechanical integrity of the individual constituents and their joints throughout the operational lifetime of the PFC is essential.
For this reason, advanced material concepts, such as W-fiber-reinforced composites, as well as optimized joining and manufacturing routes, are being pursued. These approaches will be combined with modelling in the future to understand irradiation-induced microstructural changes in the individual constituents and their consequences for mechanical properties. However, the degradation of material and interface properties under fusion-relevant neutron irradiation remains a major challenge and an open question for reliable PFC design. Current modelling approaches and experimental databases still rely largely on non-fusion-prototypic irradiation conditions, such as ion bombardment or neutron irradiation in fission reactors. For complex materials and joints, neutron irradiation is particularly important for assessing mechanical properties, because only neutrons provide the required bulk penetration and volume damage representative of component-relevant conditions. In addition, such irradiation data are essential for validating predictive computational models. Against this background, this contribution will present materials and PFC design concepts as well as planned computational model developments conducted at the Plasma Material Interaction and Components (P2W) division at the Max Planck Institute for Plasma Physics. In this context, gaps for fusion material qualification will be addressed from a neutron irradiation requirements perspective.Ponente: Hanns Gietl (Max Planck Institute for Plasma Physics) -
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Towards Fusion-Relevant Materials Qualification: Insights from the UK NEURONE Programme
The UK Atomic Energy Authority–led NEURONE programme is a multi-year initiative aimed at accelerating the development and deployment of advanced nuclear steels. Its primary objective is to fast-track the development, screening, and qualification of next-generation reduced-activation steels for both fusion and fission applications. These materials are designed to withstand the extreme conditions expected in future reactors, including high neutron flux, elevated temperatures, and long service lifetimes, while minimising long-term radioactive waste.
The programme integrates advanced modelling, experimental characterisation, mechanical testing, and irradiation campaigns to significantly reduce the time required to validate structural materials and enable their transition to industrial use.
A key element of NEURONE is the irradiation work package, which focuses on understanding radiation-induced microstructural evolution and the resulting changes in mechanical properties under fusion-relevant conditions. To date, this work has relied primarily on ion irradiation to simulate radiation damage and accelerate data generation. In parallel, neutron irradiation campaigns have been conducted at the High Flux Isotope Reactor (HFIR), and irradiation has recently commenced at BR2 to obtain engineering-relevant material properties.
These studies provide important insights into defect formation, phase stability, and hardening mechanisms, including the role of nano-oxide dispersions in enhancing microstructural stability. Ongoing efforts aim to quantify irradiation effects across a range of temperatures and doses, supported by advanced post-irradiation examination techniques. Future work will increase the dataset and strengthen its reliability.
Despite this progress, important limitations remain. Ion and fission neutron irradiation cannot fully reproduce the combined effects of displacement damage and transmutation reactions characteristic of fusion environments. In particular, the lack of high-energy neutron irradiation limits the ability to accurately assess transmutation products and their impact on long-term material performance. Addressing these challenges will require access to dedicated fusion-relevant neutron sources, such as IFMIF-DONES, which are essential for the next phase of materials qualification.Ponente: Slava Kuksenko (United Kingdom Atomic Energy Authority) -
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Study of the W-based High Entropy Alloy in DiFU as support facility for pre-selection of materials for DONES
The two processes relevant when testing a material for fusion environments are its response to (1) displacement damage and (2) transmutation reactions [1] can be mirrored by ion beam irradiation by heavy ion irradiation, and by helium implantation. The best effect can be achieved when these two types of ion irradiations are applied simultaneously in the dual-beam irradiation setup, like the Dual-Beam Ion Irradiation Facility for Fusion Materials (DiFU) at Ruđer Bošković Institute [2], which is one of only a dozen worldwide. DiFU was built at RBI as support facility for pre-selection of materials for DONES, so the chosen materials will be prepared as small bulk samples for DONES study.
For fusion applications, W and W-based alloys, especially refractory high entropy alloys (RHEA), are known as high heat flux (about 10 MW/m2) materials for plasma facing components e.g. first wall and diverter [3]. To prepare and study larger number of different compositions of alloys as candidates for fusion materials, magnetron sputtering is shown as method of choice, so we used this method to deposit WTaVCr thin films. Their structural properties and chemical composition on atomic scales were studied before and after irradiation in DiFU by dual or single beam.
WTaVCr films were deposited on a silicon substrate. Films were irradiated in DiFU with dual beam of 8 MeV Cu3+ and 200 keV He+ to dose 1 dpa and 6 dpa (for Cu3+), and with single beam of 8 MeV Cu3+ to dose 1 dpa. The films were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS) and atomic resolution scanning transmission electron microscopy (STEM), both before and after irradiation. Moreover, a highly-performant machine-learned interatomic potential [4] was employed to perform atomistic simulations of bulk and surface WTaVCr.
As-deposited WTaVCr film dominantly contains body-centered cubic (bcc) structure with a unit-cell parameter a=3.191(2) Å and interplanar distance d011=2.25 Å, and a second, minority bcc phase with unit-cell parameter a=3.126(3) Å and interplanar distance of d011=2.21 Å. While the appearance of the second phase indicates a possible phase segregation of lighter element (V or Cr), this assumption has been disproved by atomic resolution STEM imaging in combination with EDS which show that all the elements (W, Ta, V and Cr) are homogenously distributed in all the crystal grains. These results led to the conclusion that both bcc phases were the high entropy alloys lattices containing all four metals. After irradiation with dual beam in DiFU, narrower bcc phase with a unit-cell parameter a=3.126 Å becomes dominant crystalline phase, although the bcc with a=3.191 Å can still be observed. Moreover, after irradiating as-deposited sample of thickness with single beam of 8 MeV Cu ions in dose of 1 dpa we observed that it caused complete transition of the film in the bcc phase with the smaller unit cell (a=3.126(3) Å), initially found in the minority of the as-deposited samples. These results indicated that irradiation induce ordering of the crystal lattice instead of an expected increase of the defects. To elucidate the observed phenomena and confirm whether irradiation really induce the relaxation of crystal lattice, theoretical simulations of bulk and surface WTaVCr were performed. Probability of WTaVCr to form a bcc bulk crystal of unit cell length "a" was calculated using the tabGAP [5] machine-learning interatomic potential. The simulation indicated that 3.12 is the global minimum of WTaVCr BCC crystal lattice. This statement has been approved experimentally by atomic resolution STEM imaging in combination with EDS which confirmed that all the elements are homogenously distributed in bcc crystal lattice of WTaVCr. Moreover, the Rietveld refinements of XRD measurements show that the micro-strain value ε in as deposited samples was significantly larger compared to the micro-strain present in the irradiated WTaVCr having smaller unit-cell. Observed decrease in micro-strain indicates that the irradiation causes the significant reduction in number of distortions and the relaxation of deformations originally present within the as-prepared crystal lattice finally leading to the observed decrease of unit-cell parameters.
From experimental observations and theoretical analysis, we conclude that the system, as initially deposited, is located in a substrate-induced local minimum, while irradiation of the quaternary W-based alloy WTaVCr induce relaxation in thermodynamically stabile phase.
Therefore, the irradiation‑induced ordering observed in WTaVCr under dual‑beam conditions in DiFU provides a clear basis for selecting this alloy system as a promising candidate for neutron exposure in IFMIF‑DONES.
The DiFU results can identify which compositions exhibit structural stability and reduced micro‑strain under displacement damage and helium implantation, making them suitable for further investigation under fusion‑relevant neutron spectra. Based on these findings, we propose the preparation of miniature mechanical‑test specimens that would enable the assessment of the materials properties following their irradiation in IFMIF‑DONES (small scale mechanical testing samples: for tensile testing, nanoindentation etc.). These small‑scale samples, linking post‑irradiation mechanical characterization with DiFU pre‑screening and DONES neutron‑induced material evolution would ultimately support the development of W‑based RHEAs for plasma‑facing applications.Acknowledgment: The authors acknowledge financial support of Croatian Science Foundation under the project IP-2025-02-7971.
References:
[1] G. S. Was, Fundamentals of radiation materials science: metals and alloys, Springer (2007).
[2] T. Tadić, et. al. Materials 16 (3) (2023) 1144.
[3] G. Pintsuk, et. al., Fusion Engineering and Design 174 (2022) 112994.
[4] J. Byggmästar, et. al., Acta Materialia (2025) 121276.
[5] J. Byggmästar, K. Nordlund, F. Djurabekova, Phys. Rev. Materials 6 (2022) 083801.Ponente: Andreja Gajović (Ruđer Bošković Institute)
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Lunch
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Studies of functional materials and other fusion technologies Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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Functional materials and sensors in fusion environments
This contribution reviews the performance requirements and radiation-induced degradation mechanisms of functional materials intended for operation in fusion reactors, including optical elements, electrical insulators and materials used in sensing systems. Building on the activities of the EUROfusion Functional Materials group, we identify the key irradiation needs for future fusion devices and assess how they could be addressed by IFMIF-DONES.
Particular attention is given to extending irradiation experiments from bulk materials to functional elements, interfaces and small instrumented mock-ups. This is essential for validating magnetic and optical sensors, diagnostic components, and heating and control systems, whose performance also depends on cables, optical fibres and feedthroughs.
Finally, we discuss the experimental interfaces that may be required in the DONES irradiation area for the future qualification of functional components and integrated sensor systemsPonente: Dr. Rafael Vila (CIEMAT) -
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Enlarging the Perspectives of IFMIF-DONES by Neutronics Qualification of Functional Materials for the Breeding Blankets and Fusion Reactors
Responding to the growing interest from the DONES users community, this work provides a comparative neutronics assessment of key diagnostic and control components to address the critical needs of future facilities. While structural materials often dominate radiation damage discussions, functional components face unique operational limits under intense neutron fields. This paper addresses the specific challenge of evaluating these neutronics responses in a power-plant environment and maps those requirements directly to the experimental volumes and irradiation conditions provided by the IFMIF-DONES facility.
To provide a comprehensive neutronics evaluation, this study defines and analyzes key categories of functional materials:
- Tritium breeding and Neutron multiplication materials, analyzing
advanced ceramic breeder (ACB) pebbles (lithium orthosilicate with 35
mol% lithium metatitanate) and Li8PbO6 octalithium plumbate,
alongside neutron multipliers, including TiBe12 in the Helium-Cooled
Pebble Bed (HCPB) and the stagnant liquid lead of the Water-Cooled
Lead-Lithium Ceramic Breeder (WLCB) blanket concepts; - Electrical Insulators, specifically investigating MgO and Al2O3;
- LTS and HTS superconducting coil materials: Nb3Sn, REBCO, stabilizer matrix;
- Optical Elements, incorporating irradiation studies of chemical vapor deposition (CVD) diamond windows and fiber optic cables.
Comprehensive radiation transport and activation calculations were performed for both MgO and Al2O3 to evaluate their suitability in intense neutron fields. The simulations characterize the specific spatial distribution of neutron flux and fluence, nuclear heating, and neutron damage (dpa), directly comparing the irradiation conditions within the DONES High Flux Test Module (HFTM) and Medium Flux Test Module (MFTM) against the expected exposure at the DEMO First Wall (FW). Furthermore, the long-term activation behavior, decay heat profiles, and specific transmutation pathways—such as the generation of sodium (Na) isotopes—were systematically analyzed.
Neutrons degrade superconductors through lattice displacement (reducing critical temperature and critical field) and resistivity spikes in the copper stabilizer matrix due to transmutations. We analyzed the Low-Temperature Superconductor (LTS) Niobium-Tin material (Nb3Sn) defined in ITER, DEMO/VNS, and the High-Temperature Superconductor (HTS) Rare-Earth Barium Copper Oxide (REBCO) materials used in SPARC, ARC, Proxima Fusion (Stellaris concept), and Gauss-Fusion (GIGA plant). To quantify and predict resistivity spikes in the stabilizer matrix made of highly pure copper surrounding the superconductor, we calculated neutron fluence, neutron damage, and nuclear transmutation. We applied the MCNP6.2 and McDeLicious-17 radiation transport and FISPACT-II inventory codes and the actual MCNP neutronics models of DONES. The materials are irradiated by the neutron spectra of HFTM and the MFTM versions, such as the In-Situ Ceramic Breeder Irradiation Module (ICBIM) and BLanket fUnctional Materials modulE (BLUME).
Special emphasis is placed on identifying how closely the high-energy deuteron-lithium neutron spectrum can emulate the specific degradation mechanisms—such as Radiation-Induced Conductivity (RIC) in ceramic insulators and transmission loss in optical diagnostics — expected in a commercial fusion environment. Ultimately, this work quantifies the capabilities of IFMIF-DONES to accelerate the qualification of essential functional technologies, providing the fusion community with the predictive data necessary for robust engineering design finalization of breeding blankets and auxiliary systems.
Ponente: Dr. Arkady Serikov (Karlsruhe Institute of Technology (KIT)) - Tritium breeding and Neutron multiplication materials, analyzing
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DONES as a Key Infrastructure for the Validation of Advanced Fusion Coatings
Advanced coatings and permeation barriers are increasingly recognized as enabling technologies for the deployment of liquid breeder blankets in future fusion reactors. In PbLi-based systems, coatings are expected to play a critical role in mitigating corrosion, controlling tritium permeation, improving material compatibility, and extending component lifetime under the extreme thermo-mechanical and irradiation conditions foreseen in DEMO.
Recent developments in coating technologies have focused on the fabrication and optimization of oxide, ceramic and multifunctional barriers compatible with liquid breeder environments. Significant progress has been achieved in understanding coating behaviour under thermal exposure, flowing PbLi conditions and coupled corrosion-permeation phenomena. In parallel, current research is evolving toward more technologically relevant approaches, including coating integration in complex geometries, scalability of deposition methods and assessment under representative operational conditions.
Despite these advances, the qualification of coatings for fusion applications still faces major challenges due to the limited availability of irradiation facilities capable of reproducing fusion-relevant neutron spectra and damage levels. In this context, DONES will provide a unique opportunity to bridge the gap between laboratory-scale developments and reactor-oriented validation. This contribution discusses ongoing coating developments for liquid breeder applications and analyses how DONES could become a key infrastructure for their qualification through dedicated experimental campaigns.Ponente: Elisabetta Carella (CIEMAT - National Fusion Laboratory) -
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Advanced Superconducting Components and Materials Testing Laboratory at IFMIF-DONES (DONES-SCMag)
Andrzej J. Zaleski
The commercial viability of next-generation fusion reactors, such as DEMO and Fusion Pilot
Plant, relies heavily on high-field superconducting magnets. During operation, these systems
will be exposed to an unprecedented, intense flux of fast (14 MeV) neutrons, which cause severe
radiation damage, microstructural degradation, and a subsequent decline in critical parameters
Tc, Hc2, Jc.
To address this critical issue, we propose to establish DONES-SCMag, a dedicated research
facility integrated into the IFMIF-DONES infrastructure in Granada. Moving beyond standard
post-irradiation examinations (PIE), this laboratory will feature a pioneering capability for realtime,
in-operando characterization of both superconducting materials (HTS/LTS) and
functional components (e.g. prototype coils, high-current cables, and joints) directly exposed
to the neutron flux. The facility will allow continuous monitoring of the voltage-current V-I
characteristics, magnetic flux penetration, and quench dynamics under high magnetic fields and
cryogenic temperatures (4.2 K – 77 K) during on-going neutron irradiation.
A key engineering focus of the laboratory will be addressing the extreme conditions of in-situ
testing, specifically mitigating intense nuclear heating within the insertion cryostats and
monitoring the severe activation of stabilizer and structural materials (e.g. copper, silver, and
steel alloys) under the fast neutron flux.
This initiative is envisioned to be driven by a Polish-led scientific collaboration combining
expertise in low-temperature physics, materials science, and cryogenic engineering, which
could in the future form the nucleus of a broader consortium. The Institute of Low Temperature
and Structure Research in Wrocław (INTiBS), incorporating research groups specializing in
superconductivity and high magnetic fields, would take a leading role, together with potential
partners such as the Wrocław University of Science and Technology (WUST), in developing
specialized cryogenic transport systems, insertion cryostats, and advanced magnetometry. The
collaboration could be further complemented by the Institute of Nuclear Physics in Kraków
(IFJ PAN), which would contribute expertise in nuclear engineering, radiation transport
modelling, and neutron dosimetry. Such a group could subsequently seek collaboration with
leading international fusion laboratories, with the long-term aim of creating a global hub for the
validation of superconducting magnet technologies for clean energy generation.
The forthcoming presentation will detail the physical challenges associated with deploying
superconducting materials (HTS/LTS) and functional components within a fast neutron
irradiation environment. Furthermore, it will outline the critical parameters that must be
monitored to accurately characterize the degradation of their functional properties. Finally, a
conceptual design for the DONES-SCMag facility, along with a strategy for its integration into
the IFMIF-DONES infrastructure, will be proposed.Ponente: Prof. Andrzej Zaleski (ILT&SR PAS, Poland)
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Coffee break
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Life sciences and medical applications Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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IFMIF-DONES role in Personalized Nuclear Medicine
Nuclear medicine is moving steadily toward a personalized approach, driven by the development of Targeted Radionuclide Therapy (TRT) and theranostic strategies that allow diagnosis and treatment to be tailored to the molecular profile of each patient’s disease. TRT relies on radiolabeled compounds that accumulate selectively in tumors or other pathological tissue, delivering cytotoxic radiation while sparing healthy organs. Theranostics goes a step further, pairing diagnostic and therapeutic radiopharmaceuticals against the same biological target, which makes it possible to select patients, plan treatment, monitor response and calculate individualized dosimetry.
None of this reaches the clinic without solid preclinical work behind it. Animal and cellular models remain essential to evaluate biodistribution, pharmacokinetics, dosimetry, efficacy and toxicity of new radiopharmaceuticals before they move into clinical trials — this is the bridge between isotope production and the patient, and it’s where safety and efficacy actually get tested.
IFMIF-DONES, although conceived primarily for fusion research, offers a real opportunity here. Its fast neutron source — deuterons of 40 MeV hitting a liquid lithium target — reaches energies of 14–20 MeV, opening up nuclear reactions such as (n,2n) that conventional thermal reactors simply cannot access, since their energy thresholds are too low (for instance, 99Mo production via 100Mo (n,2n) requires around 8.4 MeV). This matters for medicine because these fast-neutron routes give access to isotopes such as 47Sc and 67Cu with the specific activity and isotopic purity needed for safe clinical use.
It’s also possible to divert part of the 40 MeV deuteron beam to produce other promising theranostic isotopes, like 165Er or 177Lu. This accelerator-based route is particularly relevant for reaching the high specific activity and no-carrier-added purity that efficient radiolabeling demands, so that the radioactive atoms bind to their molecular targets without competing against stable isotopes.
Taken together, IFMIF-DONES could complement existing reactor and cyclotron infrastructure and help reinforce Europe’s capacity to produce radioisotopes, securing supply for advanced imaging and targeted therapies. Access to high-quality isotopes would also benefit preclinical research at centers like CIEMAT, supporting the development of new radiopharmaceuticals and, ultimately, the progress of precision oncology and personalized medicine.
Ponente: Marta Oteo (CIEMAT) -
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Radiobiology at DONES: Current Status and Future Perspectives
Studying the effects of neutrons on the human body is a topic of great current interest. Neutrons can be regarded as a double-edged sword: depending on the context, they may pose a health risk (in occupational environments, space missions, etc.) or serve as a therapeutic tool, as in treatments such as Boron Neutron Capture Therapy (BNCT).
Despite the significant scientific interest in understanding the biological effects induced by these particles, a major limitation persists: the number of neutron facilities where biological experiments can be performed remains very scarce, and many of those currently in operation are approaching closure. Against this background, DONES represents a key opportunity, as it will enable radiobiology experiments focused on the irradiation of biological samples and the subsequent assessment of the radiation-induced damage.
Although these activities are classified within the Complementary Experiments of DONES, a comprehensive strategy for both the irradiation and the processing of biological samples within the facility is currently under development. Based on the group's experience gained at other international neutron facilities — such as the Institut Laue-Langevin (ILL) and the ISIS Neutron and Muon Source — the most suitable irradiation rooms for biological experiments at DONES have been identified. Moreover, a dedicated radiobiology laboratory ("Bio-DONES lab") has been designed, which can be located within the Main Building and will house all the instrumentation and materials required for post-irradiation sample processing.
In conclusion, the present work demonstrates the current potential of DONES for radiobiology studies and outlines future perspectives.
Ponente: Cristina Méndez Malagón (Universidad de Granada) -
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High-Power Target Technology for Deuteron-Induced Medical Radioisotope Production at IFMIF-DONES
The unique neutron environment available at IFMIF-DONES offers significant opportunities for life-science and medical applications, including radiobiological research, neutron-based therapies, and the production of radioisotopes for nuclear medicine. In particular, the growing demand for diagnostic and therapeutic radionuclides has motivated the exploration of innovative production routes that can complement existing reactor- and accelerator-based facilities [1].
Beyond neutron-induced production pathways, the high-current deuteron accelerator at IFMIF-DONES may also provide access to alternative radioisotope production schemes based on charged-particle reactions. Such an approach could enable the production of emerging and novel medical isotopes while taking advantage of the unique capabilities of the facility. A key technological challenge for the implementation of these deuteron-induced production routes is the development of target systems capable of operating under the extreme thermal loads generated by high-intensity deuteron beams while maintaining structural integrity and reliable performance.
To address this challenge, the University of Granada has developed an innovative high-power target technology specifically conceived for applications intense charged-particle beams. The concept combines enhanced heat-removal capabilities with robust thermo-mechanical design, enabling efficient operation under beam power densities relevant to next-generation accelerator facilities. Such characteristics make this technology particularly attractive for future medical isotope production systems associated with high-current deuteron accelerators.
In this work, we present the first experimental validation of this technology performed within the framework of a collaboration between the University of Granada and the Laboratoire de Physique Subatomique et de Cosmologie (LPSC, Grenoble, France). Irradiation tests were carried out at the LPSC high-power electron beam facility to assess the thermal dissipation capability and structural robustness of the target under representative operating conditions [2]. Experimental results are compared with Monte Carlo particle transport simulations and thermo-mechanical calculations developed for the target design.
The potential application of this technology to deuteron-induced medical isotope production at IFMIF-DONES is discussed through two representative case studies. The theranostic radionuclide 177Lu, one of the most relevant radioisotopes for targeted radionuclide therapy, along with its SPECT imaging capabilities [3-5], and the emerging therapeutic radionuclide 165Er from natural holmium targets [6,7] is also considered as a complementary example. The results demonstrate the feasibility of advanced high-power target concepts for future medical isotope production systems and highlight a promising pathway to expand the scientific and societal impact of IFMIF-DONES beyond its primary fusion mission.
Ponente: María Elena López Melero (University of Granada)
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Neutron irradiation of electronics and other industrial applications Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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CNA as a Combined Irradiation Testing Center: Fostering Academia and Industry Symbiosis
As a recognized Unique Scientific and Technical Infrastructure (ICTS) in Spain, the Centro Nacional de Aceleradores (CNA) is a joint research center operating under the Universidad de Sevilla, the Spanish Research Council (CSIC), and the Andalusian Regional Government. Having pioneered irradiation testing within the country, the infrastructure offers open-access capabilities to both public and private entities. The center has not only strengthened its research and commercial services portfolios but has also established a two-way transfer of knowledge.
The irradiation unit of the CNA coordinates all the research related to reliability testing on devices and materials that could be used in critical radiation environments, such as the space environment or high energy Physics experiments. As well as the irradiation of materials that implies their internal modification for applications in agriculture, medicine or biology. This type of test, in static and/or dynamic mode, is performed in RadLab using gamma photons and in the laboratories of Tandem and Cyclotron particle accelerators.
Last year’s escalating demand for Commercial Off-The-Shelf (COTS) and radiation-hardened electronic components in the Aerospace and High Energy Physics sectors has intensified the need for accessible, reliable, and versatile irradiation testing facilities. The CNA is strongly committed to participating in the European applied physics facilities networks. By adapting academic research infrastructure to meet strict industrial standards, CNA not only drives technological innovation but also provides these sectors with an efficient, high-fidelity testing ground to guarantee functional reliability.
This presentation focuses on our group activities related to the effects of radiation on electronics, as well as on the capabilities of the CNA as a combined irradiation testing facility. In addition, we will review some key aspects for facilities design and development, highlighting the compliance with the main radiation specifications and guidelines.Ponente: YOLANDA MORILLA GARCIA (CNA (US / CSIC / JA)) -
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Synergies HiSPANoS-DONES: Recent user experiments at HiSPANoS and plans for the new compact 14 MeV DT generator
In the context of production and use of accelerator-driven neutrons, Spain hosts the CNA HiSPANoS neutron source in Sevilla. Currently, HiSPANoS produced continuous and pulsed beams of thermal, epithermal and fast neutrons which are used for many different applications, including nuclear physics experiments and industrial applications. Recently, with the support of IFMIF-DONES, the Spanish government has granted the funds necessary to expand the portfolio with a compact DT generator of 14 MeV neutrons, aiming at yields in the 1e9-1e10 n/s range.
The installation, commissioning and use of the HiSPANoS DT generator offers a unique opportunity for the preparetory work of the commissioning of DONES R-160 and as test-bench for the proposed experiments with continuous beams.Ponente: Carlos Guerrero (Universidad de Sevilla / Centro Nacional de Aceleradores (CNA)) -
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Characteristics of the neutron source at the entrance to the DONES Complementary Experiments Room R160
For neutron experiment planning inside the DONES Complementary Experiments Room 160 (CER R160), it is necessary to estimate the variability of the CER R160 neutron source, which is formed by neutrons collimated through the Neutron Beam Tube and Shutter (NBT&S). In the Third DONES Users Workshop 1, we demonstrated the neutron source's dependence on the number and design of the irradiation test modules installed inside the Test Cell (TC). We considered the HFTM and two types of MFTM (BLUME and ICBIM) with the objective of minimizing the impact of the TC modules on neutrons entering the CER R160. In this work, we formulate the concept of neutron source synergy, which amplifies the usability of DONES through the effective distribution of neutrons among several irradiation modules and experiments located in both the TC and the CER. For this Workshop, we provide the results of a study on neutron flux growth at the CER entrance resulting from an increased NBT&S aperture diameter. Additionally, we analyzed modifications to the NBT&S neutron beam-line orientation for extended DONES operation at 250 mA with two accelerators running. The results of these feasibility studies for neutron beam redirection and tube diameter optimization are critical to discuss with potential users setting up neutron experiments in the CER.
The effect of neutron flux growth due to a larger tube diameter depends heavily on the size of the prospective experiments in the CER. The performed parametric analysis showed a quadratic dependence of the total neutron flux on the tube aperture size for a detector with a 30 cm diameter (D30) at the CER entrance. For this fixed-size D30 detector, doubling the tube diameter from D15 to D30 resulted in a 4.44-fold increase in the total neutron flux, while a square root of 2 (1.414) diameter increase from D15 to D21 yielded a 2.01-fold increase. The diameter D21 was chosen because 1.414×15≈21.2. Conversely, if the CER detector is smaller and scaled to match the collimated tube diameter, the neutron flux dependence on the tube diameter is weaker: increasing from D15 to D30 yields only a 1.25-fold flux increase, and an increase from D15 to D21 yields just a 1.13-fold increase. To finalize the engineering implementation of the NBT&S design, feedback from potential users planning neutron experiments in the CER is highly valuable.
References:
1 A. Serikov et al., “Updates on the BLUME and TRTM OIMs impact on the collimated neutrons entering Complementary Experiments Room R160 at DONES”, Third DONES Users Workshop, Zagreb, Croatia, October 1-2, 2024, https://indico.ifmif-dones.es/event/29/contributions/793/Ponente: Dr. Arkady Serikov (Karlsruhe Institute of Technology (KIT))
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Workshop Dinner
Conference Dinner for workshop participants at the Restaurant Stari Fijaker, Mesnička Street No. 6, Zagreb
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DONES users community: presentation of the Users Committee members and future activities Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid -
Experiments during the commissioning phase of DONES Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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Current Status of the European TBM Project and a Possible Use of DONES for Preliminary Testing
The European Test Blanket Module (TBM) programme is a key element of the European fusion roadmap, aiming to demonstrate tritium breeding and heat extraction technologies under fusion-relevant conditions and to support the development of future DEMO breeding blanket systems. Significant progress has been achieved in recent years in the design, safety assessment, manufacturing qualification and integration of the European Water-Cooled Lithium Lead (WCLL) and Helium-Cooled Ceramic Pebble (HCCP) TBM concepts. Ongoing activities focus on design consolidation, safety demonstration, component fabrication, validation of manufacturing routes, material characterization, and the preparation of dedicated experimental campaigns to support licensing and future deployment in ITER.
Despite these advances, several critical challenges remain, particularly related to neutron-induced material degradation, tritium behaviour, instrumentation performance, and thermo-mechanical response under fusion-relevant irradiation conditions. The availability of the IFMIF-DONES facility could provide a unique opportunity to investigate these phenomena under a neutron spectrum representative of future fusion power plants and to generate qualification data for materials and technologies relevant to breeding blanket systems.
This contribution presents an overview of the current status of the European TBM project, with emphasis on outstanding irradiation-related challenges and qualification needs. Potential opportunities for utilizing DONES during its early operational phases are discussed. Preliminary testing activities could include irradiation of structural and functional materials, breeder and multiplier materials, tritium permeation barrier concepts, instrumentation components, and small-scale mock-ups representative of TBM systems. Such experiments would contribute to reducing technological risks, validating predictive models, and preparing a comprehensive irradiation programme supporting both ITER TBM exploitation and the development of DEMO breeding blankets.
Finally, the paper discusses potential synergies between the European TBM programme and the DONES user community, and outlines candidate experimental campaigns aligned with the pre-DEMO technology qualification strategy.Ponente: Milan Zmitko (Fusion for Energy - External Expert) -
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Qualification of EUROFER97 within EUROfusion: supporting material validation strategies for IFMIF-DONES and future fusion power plants
EUROFER97 reduced activation ferritic-martensitic (RAFM) steel is the European reference structural material for breeding blanket applications in future fusion power plants. Its qualification, together with that of its welded joints, under representative fusion operating conditions is a key step towards the deployment of reliable structural components capable of withstanding high neutron fluxes, elevated temperatures and complex thermo-mechanical loading conditions.
EUROfusion’s Work Package “Materials” and Fusion for Energy (F4E) have identified the qualification of EUROFER97 and its welded joints as one of the major objectives for the 2021–2027 period. The programme aims to support the ITER-TBM programme through the integration of EUROFER97 into the RCC-MRx code while validating the mechanical behaviour and structural design methodologies required for fusion nuclear technologies. Activities currently underway include low cycle fatigue, creep, fracture toughness and fatigue crack growth testing, together with neutron irradiation campaigns covering temperatures between 275 °C and 550 °C and irradiation doses up to 2 dpa.
The experimental results obtained so far provide important input for the qualification of structural design methodologies relevant to breeding blanket systems and future fusion facilities. In particular, the programme contributes to the assessment of engineering rules addressing ratcheting, creep-fatigue interaction and irradiation-induced plastic flow instability under fusion-relevant conditions. In parallel, the ongoing activities are helping to develop irradiation strategies, testing procedures and post-irradiation examination methodologies that are directly relevant for the future operation of IFMIF-DONES.
This contribution presents an overview of the qualification activities performed during the 2021–2025 period and discusses their relevance for reducing material performance uncertainties in future fusion environments. The experimental database and engineering knowledge generated within the programme represent an important step towards the qualification of structural materials for future fusion power plants, while also providing valuable guidance for the future exploitation of IFMIF-DONES as a fusion-oriented neutron irradiation facility.Ponente: Marta Serrano Garcia (CIEMAT)
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Coffee break
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Tritium breeding technologies: validation at DONES Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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IFMIF-DONES as a key facility for HEXA breeding blanket qualification
Gauss Fusion is an industrial fusion company based in Garching, Germany. The company is developing the system architecture and critical enabling technologies required to make fusion power plants buildable, maintainable and deployable. “GIGA”, Gauss Fusion’s gigawatt-class fusion power plant concept, provides the architecture baseline to enable a targeted integrated framework for identifying, validating and maturing systems required for fusion development.
Gauss Fusion is advancing proprietary technologies that address critical constraints in fusion power plant design, integration and operation. A key programme under development is “TRIMAT”: an enabling technology platform and tritium ecosystem covering industrialised material choices (IMAT) and integrable tritium technologies (TRI). This includes HEXA tritium breeding blankets with interfacing tritium and heat extraction systems, applicable to any fusion device concept, and the wider HELIOS tritium fuel cycle for stellarators.
IFMIF-DONES is a significant facility in the HEXA breeding blanket qualification strategy to contribute to achieving TRL-6. From a user’s perspective, two significant outcomes are foreseen using the facility. On the one hand, IFMIF-DONES may act as a qualifying platform, enabling partial integration testing to demonstrate HEXA breeding blanket functions and, therefore, supporting TRL progression. On the other hand, IFMIF-DONES will act as a substantiation device, to obtain material properties under relevant fusion neutron irradiation that will enable End-Of-Life assessments of baseline reactor materials for GIGA. To facilitate the leveraging of IFMIF-DONES for these two critical development programs, it is essential that the facility has the relevant volume and environmental conditions (multiple effects and neutron fluence) for prototype testing, and the appropriate supporting auxiliary systems.
Ponente: Sr. Jacobo Zegrí Reiriz (Lead of Tritium Breeding Blanket at Gauss Fusion GmbH) -
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Recent Progress in Kyoto Fusioneering's R&D on Fusion Blanket Components and Materials for IFMIF-DONES Testing
In the development of breeding blankets for fusion power plants, it is crucial to create material irradiation environments that reproduce fusion-relevant neutron spectra and fluences. IFMIF-DONES will provide an irradiation environment with neutron energies and fluxes relevant to fusion applications, enabling the assessment of materials and components under conditions closer to those expected in future fusion power plants.
Various structural materials are being developed for fusion power plant breeding blankets, including reduced-activation ferritic/martensitic (RAFM) steels, V-alloys, and SiCf/SiC composites. Kyoto Fusioneering (KF) is conducting R&D on these materials, focusing on their interactions with several liquid metal and molten salt coolants, and the effects of neutron irradiation. Since most available irradiation data originate from fission neutron environments, evaluation of material-coolant systems under fusion-relevant environments at IFMIF-DONES is essential.As one of blanket type, KF's Self-Cooled Yuryo Lithium-Lead Advanced (SCYLLA©) used SiCf/SiC structural material [1] is presented. Recent progress in the blanket are engineering designs, neutronics performance and tritium extraction technologies. In addition, it is conducted the R&D works on the material compatibility of SiCf/SiC. Focus is given to ongoing design maturation activities, including remote handling considerations, manufacturability assessments, and developments aimed at supporting future demonstration-relevant blanket testing and commercial fusion deployment. Through the discussion of neutron irradiation experimental plannings for SiCf/SiC components intended for SCYLLA, it will be established methodologies that can also be applied to other materials, such as RAFM and V-based alloys.
Numerical simulation works of a Neutron Source Package for OpenMC under DONES Irradiation target are also conducted. The source code has been generated from detailed deuterium (D)-lithium (Li) cross-sectional area calculations independently performed using PHITS + JENDL/DEU-2020 and MCNP6 + McDeLicious, and is presented alongside a simple benchmark exercise. The results demonstrate that the strong correlation between neutron energy and emission angle with respect to the Li target can be successfully reproduced in OpenMC, enabling representative IFMIF-DONES neutronics simulations with a practical level of accuracy, based on a joint collaboration by IFMIF-DONES Spain, KIT, and KF.
Keywords: IFMIF-DONES; fusion blanket; SCYLLA; lithium-lead; SiCf/SiC composites; neutron irradiation; tritium extraction; materials compatibility; neutronics modelling; OpenMC.
[1] L. Candido et al., “Preliminary design of the self-cooled lithium-lead SCYLLA blanket for a spherical tokamak,” Fusion Engineering and Design, vol. 223, Art. no. 115574, Dec. 2025, doi: 10.1016/j.fusengdes.2025.115574.
Ponente: Sr. Mario Oliver (Kyoto Fusioneering UK Ltd.) -
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TBU-WCLL radiation parameters assessment on IFMIF-DONES facility
The Water-Cooled Lithium-Lead (WCLL) Breeding Blanket (BB) is one of three concepts actively developed by EUROfusion as driver blanket candidates for the EU Fusion Demonstration Plant (EU-FDP). This reference design employs liquid PbLi eutectic as breeder material and water as coolant, integrated with EUROFER structures. Despite significant design progress, critical technologies—including PbLi/EUROFER compatibility, tritium management systems, and thermo-mechanical behavior—require qualification under genuine fusion neutron irradiation.
To achieve this qualification, ENEA and CIEMAT have established a collaborative effort to design and develop a Water-Cooled Lithium-Lead Test Blanket Unit (WCLL-TBU) for irradiation testing at the International Fusion Materials Irradiation Facility – Demo Oriented Neutron Source (IFMIF-DONES). The TBU-WCLL targets a neutron irradiation environment representative of the WCLL EU-FDP breeder zone.
This work presents a sensitivity study of irradiation effects on WCLL-TBU materials considering the first conceptual design, as a function of different IFMIF-DONES Test Cell configurations. Parametric analyses identified optimal configurations that maximize tritium breeding performance, irradiation uniformity, and damage metrics. This study provides clear guidance on the most appropriate Test Cell configurations to achieve optimal irradiation conditions for validating breeding blanket technology under FDP-relevant neutron environments.Ponente: Fernando Mota (Laboratorio Nacional de Fusión, CIEMAT) -
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LBVM geometrical configuration for permeation control optimization
One of the most relevant objectives of the Liquid Breeder Validation Module is the study of tritium permeation through structural materials considered for future nuclear fusion power plants, as well as the effect of permeation barriers applied to these materials.
Permeation is mainly affected by the temperature of the wall through which it occurs, following Arrhenius-type relationships. Therefore, temperature control is of utmost importance in order to maintain high temperatures at surfaces where permeation is desired, while keeping low temperatures at other surfaces intended to act as confinement barriers.
On the other hand, a capsule design for the module should be as compact as possible, so that the largest possible number of capsules can be accommodated, thus maximizing the utilization of the irradiation volume available in the Test Cell of IFMIF DONES.
The geometric configuration, including capsule dimensions, experimental tube geometry, and container dimensions, together with purge He and cooling He flow rates involves multiple design requirements. These include consideration of different heat transfer mechanisms (conduction, convection, and radiation), as well as a realistic and adjustable electrical power input.
The presentation will describe the considered factors, boundary conditions, governing equations, and the results obtained.Ponente: FERNANDO ARRANZ (CIEMAT) -
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Nuclear Reaction Analysis as a Qualification Tool for Hydrogen Isotope Retention in Lithium-Based Functional Materials for Fusion Applications
The development of fusion reactors beyond ITER requires the qualification of functional materials capable of operating under intense particle and neutron irradiation while maintaining their structural and functional properties. Lithium-based materials are attracting increasing interest for advanced fusion technologies, including liquid-metal plasma-facing concepts [1], due to their ability to mitigate power loads and reduce impurity contamination. However, their strong affinity for hydrogen isotopes may significantly affect fuel retention, material performance, and operational safety.
Accurate quantification of deuterium retained in lithium-containing materials is therefore essential for assessing their suitability under fusion-relevant conditions. Nuclear Reaction Analysis (NRA) using the ²H(³He,p)⁴He reaction [2,3] is one of the most sensitive techniques for hydrogen isotope measurements. Nevertheless, the presence of lithium introduces competing nuclear reactions whose emitted particles partially overlap with the deuterium signal, potentially limiting the detection capability.
In this work, the sensitivity limits of NRA for deuterium quantification in lithium-based materials were investigated using a Li-Sn alloy containing 15 at.% Li implanted in situ with 10 keV deuterium ions up to a fluence of 10¹⁷ions/cm². Measurements performed with a 2.3 MeV ³He beam demonstrate that the interference from lithium-induced reactions does not compromise reliable deuterium quantification. The detection limits obtained for the alloy are discussed and extrapolated to pure lithium systems.
These results highlight the capability of ion-beam analysis techniques to support the qualification of lithium-based functional materials for future fusion reactors. The methodology is directly relevant for studying hydrogen isotope retention and irradiation-induced effects in materials expected to operate under DEMO and IFMIF-DONES relevant environments.[1] F.L. Tabarés, Plasma Phys. Control. Fusion 58 (2016) 014014
[2] J.P.S. Loureiro et al., Nucl. Mater Energy 12 (2017) 709
[3] R. Mateus et al., Nucl. Instrum. Methods Phys. Res. B 486 (2021) 55Ponente: Dr. Norberto José Sobral Catarino (IPFN, University of Lisbon, Instituto Superior Técnico)
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Lunch
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Other experiments and facilities relevant for DONES Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid-
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Structural and environmental compatibility of 316L/316Ti–EUROFER97 TIG welds for DONES Target Assembly Backplate
Dissimilar welds between austenitic stainless steels and EUROFER97 are unavoidable in the DEMO Oriented Neutron Source (DONES) Target Assembly (TA), particularly in the Backplate (BP), where 316L/316Ti piping joins EUROFER97 structural components exposed to extreme neutron flux, lithium velocity and thermal gradients that drive BP lifetime. This work assesses thin TIG (GTAW) butt welds in 1G configuration without filler on 2 mm plates, establishing a unified framework for the structural integrity and liquid lithium compatibility of BP relevant joints.
A 316L–316L reference campaign validated the welding configuration and identified the optimal current window balancing penetration, internal defects and heat affected zone (HAZ) extension. Radiographic inspection showed evolution from lack of fusion at low current (32-34 A) to porosity at high current (45-55 A), with 38-42 A providing the best continuity/porosity compromise. Optical microscopy, SEM and EBSD confirmed austenitic solidification with minor delta ferrite and the equiaxed-to-directionally solidified transition, while room temperature tensile tests and Vickers hardness profiling (200 gf) established the mechanical baseline.
Dissimilar 316L–EUROFER97 and 316Ti–EUROFER97 BP representative coupons required higher current (≈65 A) for stable fusion due to EUROFER's distinct thermal properties. Metallographic examination and hardness traverses revealed pronounced microstructural/hardness gradients at ferritic–austenitic interfaces, emphasizing robust preparation/etching needs.
The assessment matrix includes radiographic inspection, EBSD phase/texture mapping across interfaces, and tensile testing for joint level strength, ductility and fracture location. Corrosion performance is evaluated through dedicated liquid lithium exposures (ELIOS-CIEMAT) in sealed AISI 316L containers with high purity Li, assembled in inert atmosphere glovebox, pressurized to 5 bar Ar, heated up to 350 °C, and operated under controlled T/P with real time SCADA monitoring. As welded and Li exposed specimens undergo identical microstructural (optical/SEM/EBSD) and mechanical (tensile/hardness) characterization, enabling direct comparison and quantitative appraisal of DONES TA Backplate dissimilar TIG weld integrity under structural and lithium breeder conditions.Ponente: Nerea García Rodríguez (CEIMAT) -
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Test and Validation of a Neutron Measurement System based on Thin-foil Proton Recoil at the DONES Neutron Source
One of the key characteristics of a neutron source is the energy spectrum of emitted neutrons. This allows, for example, inferences about the activation of various materials used to irradiate samples composed of different nuclear isotopes. In the case of fusion reactors, however, it is possible to determine basic parameters of the reactor fuel, i.e., the plasma, such as the Ti ion temperature or the fuel ion ratio nT/nD. Among the available techniques, a promising approach to neutron spectrometry in neutron environments relevant to intense neutron sources is the thin-film proton recoil (TPR) method. The proposed system is based on the detection of recoil protons generated in a thin hydrogen-rich converter exposed to the incident neutron beam. By measuring the energy and angular distribution of recoil protons, the incident neutron spectrum can be reconstructed and compared with the Monte Carlo prediction. Currently, the high-resolution neutron spectrometer based on the TPR method is under development at IFJ PAN in Kraków [1 - 3].
This contribution presents a proposal for testing and validating a neutron measurement system during the commissioning and early operation phases of DONES. The proposed tests focus on several key aspects, such as selection of the most optimal detectors, optimization of the geometry stand, verification of detector response under realistic DONES neutron flux conditions, assessment of neutron energy reconstruction capabilities, and benchmarking of simulation models against experimental data. Particular attention will be given to the expected 14 MeV neutron component and to the influence of scattered neutrons originating from surrounding structures.
The campaign is intended to provide an experimental basis for qualifying TPR diagnostics as a neutron spectrometry tool for future fusion neutron facilities. The results will contribute to the development of robust neutron monitoring methodologies and support the establishment of validated diagnostic systems for high-intensity fusion-relevant neutron sources. Similar measurements will be possible and planned for other neutron diagnostic concepts. This will enable the qualification and characterization of the parameters of fusion neutron diagnostic systems designed using numerical modelling.
References
[1] M. Scholz, et al., Neutron spectrometer based on a gas electron multiplier (GEM) detector for fusion reactors, Fusion Eng. Des., 222 (2026) 115480, doi: 10.1016/j.fusengdes.2025.115480,
[2] A. Jardin, et al., GEM detector as a neutron spectrometer for fusion plasmas: some modelling and design aspects, . Instr., 20 (2025) C04015, doi: 10.1088/1748-0221/20/04/C04015,
[3] J. Dankowski, et al.,Development and performance of the thin-foil proton recoil spectrometer for ITER plasma diagnostics, Fusion Eng. Des., 219 (2025) 115263, doi: 10.1016/j.fusengdes.2025.115263,
Acknowledements
This work has been carried out within the framework of the EUROfusion Consortium, funded by the European Union via the Euratom Research and Training Programme. This work was done as part of a project co-financed by ITER Organization, France. Views and opinions expressed are, however, those of the author(s) only and do not necessarily reflect those of the European Union, European Commission or ITER Organization. Neither the European Union, European Commission, nor the ITER Organisation can be held responsible for them. This project is co-financed by the Polish Ministry of Education and Science in the framework of the International Co-financed Projects (PMW) program. We gratefully acknowledge Polish high-performance computing infrastructure PLGrid (HPC Center: ACK Cyfronet AGH) for providing computer facilities and support within computational grant no. PLG/2025/018826.Ponente: Dr. Urszula Wiącek (Institute of Nuclear Physics Polish Academy of Sciences, Radzikowskiego 152, PL-31342 Krakow, Poland) -
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Dual-beam facility for advanced emulation of neutron-induced damage in nuclear materials using ions
Developing next-generation nuclear technologies, including fusion (ITER, DEMO) and Generation IV reactors, requires a precise understanding of material degradation under intense fast neutron fluxes. Degradations involve atomic displacement damage (dpa) and gas production (such as H or He) via transmutation, which trigger hardening, swelling, and embrittlement. Due to the limitations of fission reactor testing, such as long irradiation time, low damage levels and sample activation, ion beam emulation has become an essential tool for rapid material qualification.
The Dual Beam Ion Irradiation Facility for Fusion Materials (DiFU) at the Ruđer Bošković Institute (Zagreb, Croatia) is one of the few multiple-beam facilities, providing dual-beam irradiation capability to the global nuclear research community.
DiFU utilizes a 6 MV Tandem Van de Graaff and a 1 MV Tandetron, equipped with SNICS and duoplasmatron sources to provide a wide range of ion species. It enables simultaneous heavy-ion and light-ion irradiation where parameters (including ion energy, dose, irradiation area, and temperature) are precisely adjusted to match specific reactor conditions. To facilitate post-irradiation analysis, the facility utilizes energy degraders to widen the ion range, creating a broader and more homogeneous irradiation volume. Furthermore, the system can achieve controlled dose and temperature gradients across a single sample, allowing for multiple data points of material response per single irradiation.
DiFU is highly adjustable for various purposes, including the study of fusion fuel blankets, plasma-facing components, and Gen IV structural materials. Operating at temperatures up to 1000 °C under high vacuum ($10^{-8}$ mbar), the facility provides an accelerated, non-activating method to study the synergy between displacement damage and transmutation products. By offering high-throughput capabilities and precise control over the irradiation environment, DiFU serves as a critical asset for the development of resilient materials for the future nuclear fuel cycle.Ponente: Mario Matic (Ruder Boskovic Institute) -
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Lithium-6: fuel for future D-T fusion power plants
By 2040, at least 100 tonnes of isotopically pure lithium-6 will be required to fabricate breeder blankets for STEP (Spherical Tokamak for Energy Production), the UK’s prototype fusion power plant. There is no currently established supply chain or large-scale lithium isotope enrichment plant to provide the needed quantities of lithium-6.
The industrially proven process for lithium-6 enrichment, COLEX (COLumn EXchange), requires massive quantities of liquid mercury that come with problematic handling issues, hazardous environmental and health implications. Alternative methods with similar separation performance such as liquid-liquid extraction have only been tested at a laboratory scale and lack trials for successful industrial-scale deployment.
This project aims to deliver a mercury-free liquid-liquid solvent extraction method using crown ethers to produce enriched lithium at the scale needed for breeder blanket manufacturing. The best-performing lithium enrichment liquid-liquid extraction system has been identified and the extraction conditions optimised.
Lithium-6 enrichment by liquid-liquid extraction has not been studied in detail and there is a poor understanding of the chemistry, making this research a valuable contribution to the field of liquid-liquid extraction, in addition to facilitating the deployment of fusion power plants.Ponente: Magali Rego (The University of Manchester) -
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RF Timer Based Photoelectron Emission Spectrometer
We propose a novel RF Timer based photoelectron emission spectrometer designed for the study of the energy and temporal characteristics of very low energy photoelectrons. In the near threshold regime, emitted electrons have kinetic energies from a few meV to several hundred meV, making their distributions highly sensitive to the work function, surface condition, electronic states near the Fermi level and defect related modifications of the material. The instrument combines very low photon energy photoelectron spectroscopy with RF Timer based electron timing, enabling measurement of photoelectron energy and photoelectron emission time characteristics in the picosecond regime.
A particularly relevant application is the characterization of neutron irradiated materials in the context of IFMIF-DONES and future fusion material qualification programs. Radiation induced vacancies, interstitials, defect clusters and surface modifications can alter the density of states, work function, carrier transport and low energy electron emission properties. By measuring both the low energy photoelectron spectrum and emission time distribution, the proposed instrument could provide complementary information on defect related electron dynamics and radiation damage.Ponente: Dr. Hasmik Rostomyan (A.I. Alikhanyan National Science Laboratory) -
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Water in cement: molecular-scale insights from neutron scattering
Water plays a central role in the mechanical strength, durability, carbonation dynamics, and ion-driven degradation in cementitious systems. Yet the structure and dynamics of water within the poorly crystalline, nanoporous main binder phases of cement, especially in the newly emerging low-CO₂ cements, are difficult to characterize by conventional techniques. Neutron scattering offers unique advantages: its high sensitivity to hydrogen, combined with H/D isotopic contrast, makes it well suited to probing water at mineral interfaces on the molecular scale. Particularly useful is the complementary use of neutron diffraction with isotopic substitution (NDIS) and inelastic incoherent neutron scattering (IINS). The former provides element-selective resolution of interfacial water ordering, a level of structural detail inaccessible to X-ray diffraction alone. Combined with molecular dynamics simulations, NDIS can reveal distinct wet and dry surface domains and identify water-surface cation coordination as water organizes at cement surfaces. The latter characterizes water dynamics through the vibrational density of states, resolving transitions from surface-adsorbed multilayer water to capillary-condensed ice-like phases—features that calorimetric or spectroscopic methods capture only partially. Together, NDIS and IINS provide a molecularly resolved picture of interfacial water, contributing to a more detailed understanding of the role water plays in governing the performance and durability of cementitious materials.
Ponente: Alexander Van Driessche (IACT-CSIC)
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Coffee break
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Discussion of the DONES experimental programme proposal Main Auditorium
Main Auditorium
CIEMAT
Venue: CIEMAT, Madrid
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